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3. The hydride H atom was revealed in the difference Fourier map and refined isotropically. The experiment was repeated with a different crystal, giving the same geometry (including the disorder and the location of the hydride ligand) within experimental error. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-151581 (1) and CCDC-151582 (2). Copies of the data can be obtained free of charge on application to CCDC. 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+ 44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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