Novel Iridaboranes from the Reactions of Cp °2Ir2HxcCl4-x, x = 0-2, with LiBH4. Existence of a Concurrent Reaction Channel in the Conversion of Metal Chlorides to Metal Hydrides

Organometallics

Volumn 18, Issue 12, 1999, Pages 2294-2296

  Lei, Xinjian ^a   Bandyopadhyay, Ananda K ^a   Shang, Maoyu ^a   Fehlner, Thomas P ^a  

^a UNIVERSITY OF NOTRE DAME   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000594816     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om990091c     Document Type: Article

References (32)

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25. max = 05.02°, Rl = 0.0475, wR2 = 0.1067 for 3665 observed unique reflections (I > 2σ(I)) and Rl = 0.0822, wR2 = 0.1324 for all 5127 unique reflections including those with negative intensities.
26. 3IrO: C, 33.45; H, 5.61. Found: C, 34.36; H, 5.78.
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28. 2: C, 35.09; H, 5.60. Found: C, 35.18; H, 5.51.
29. max = 50.02°, Rl = 0.0389, wR2 = 0.0963 for 3201 observed unique reflections (I > 2σ(I)) and Rl = 0.0503, wR2 = 0.1013 for all 4006 unique reflections including those with negative intensities.
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