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6 to 50 °C resulted in decomposition
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6 to 50 °C resulted in decomposition.
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Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon, Elsevier Science Ltd.: Oxford, Chapter 8.2
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3-allyl complexes with a single terminal substituent, the conformer with the substituent on the same side as the hydrogen on the center carbon is described as syn and the one with the substituent trans to the hydrogen on the center as anti. The syn conformer is generally more stable than the anti conformer. In order to minimize allylic strain between substituents at the ends of the allyl, the sterically demanding substituent is located at a syn rather than an anti position. (Harrington, P. J. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon, Elsevier Science Ltd.: Oxford, 1995; Vol. 12, Chapter 8.2, pp 797-904.
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We thank one of the referees for this suggestion
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