Dinuclear Complexes of Di-, Tri-, and Mixed-Valent Samarium Supported by the Calix-tetrapyrrole Ligand

Organometallics

Volumn 19, Issue 5, 2000, Pages 817-823

  Dubé, Tiffany ^a   Gambarotta, Sandro ^a   Yap, Glen P A ^a  

^a UNIVERSITY OF OTTAWA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000556557     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om9908783     Document Type: Article

References (80)

1. (a) Molander, G. A.; Hoberg, J. O. J. Org. Chem. 1992, 57, 3266.
2. (b) Jeske, G.; Jauke, H.; Mauermann, H.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8111.
3. (c) Evans, W. J.; Bloom, I.; Hunter, W. E.; Atwood, J. L. J. Am. Chem. Soc. 1983, 105, 1401.
4. (a) Li, Y.; Marks, T. J. J. Am. Chem. Soc. 1996, 118, 9295.
5. (b) Li, Y.; Marks, T. J. Organometallics 1996, 15, 3770.
6. (c) Li, Y.; Marks, T. J. J. Am. Chem. Soc. 1996, 118, 707.
7. (d) Gagné, M. R.; Nolan, S. P.; Marks, T. J. Organometallics 1990, 9, 1716.
8. (a) Takahashi, T.; Hasegawa, M.; Suzuki, N.; Saburi, M.; Rousset, C. J.; Fanwick, P. E.; Nagishi, E. J. J. Am. Chem. Soc. 1991, 113, 8564.
9. (b) Fu, P. F.; Bard, L.; Li, Y.; Marks, T. J. J. Am. Chem. Soc. 1995, 117, 7157.
10. (c) Molander, G. A.; Julius, M. J. Org. Chem. 1992, 57, 6347.
11. (a) Bijpost, E. A.; Duchateau, R.; Teuben, J. H. J. Mol. Catal. 1995, 95, 121.
12. (b) Harrison, K. N.; Marks, T. J. J. Am. Chem. Soc. 1992, 114, 9220.
13. (a) Thompson, M. E.; Bercaw, J. E. Pure Appl. Chem. 1984, 56, 1.
14. (b) Burger, B. J.; Thompson, M. E.; Bercaw, J. E.; Cotton, W. D. J. Am. Chem. Soc. 1990, 112, 1566.
15. (c) Parkin, G.; Bunel, E.; Burger, B. J.; Trimmer, M. S.; van Asselt, A.; Bercaw, J. E. J. Mol. Catal. 1987, 41, 21.
16. (a) Molander, G. A.; Nichols, P. J. J. Am. Chem. Soc. 1995, 117, 4415.
17. (b) Molander, G. A.; Hoberg, J. O. J. Am. Chem. Soc. 1992, 114, 3123.
18. (a) Marks, T. J., Fragala, I. L., Eds. Fundamental and Technological Aspects of Organo-f-Element Chemistry; D. Reidel: Dordrecht, The Netherlands, 1985.
19. (b) Schumann, H. Angew. Chem., Int. Ed. Engl. 1984, 23, 474.
20. (c) Evans, W. J. Polyhedron 1987, 6, 803.
21. (d) Evans, W. J. J. Organomet. Chem. 1983, 250, 217.
22. Ephritikhine, M. Chem. Rev. 1997, 97, 2193.
23. (a) Jeske, G.; Lauke, H.; Mauermann, P. N.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8091.
24. (b) Jeske, G.; Schock, L. E.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8103.
25. (c) Watson, P. L.; Parshall, G. W. Acc. Chem. Res. 1985, 18, 51.
26. See for example: (a) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865. (b) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283 and references therein. (c) Evans, W. J. Adv. Organomet. Chem. 1985, 24, 131 and references therein. (d) Kagan, H. B.; Namy, J. L. In Handbook on the Physics and Chemistry of Rare Earths; Gschneider, K. A., Eyring, L., Eds.; Elsevier: Amsterdam, 1984; Chapter 50.
27. See for example: (a) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865. (b) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283 and references therein. (c) Evans, W. J. Adv. Organomet. Chem. 1985, 24, 131 and references therein. (d) Kagan, H. B.; Namy, J. L. In Handbook on the Physics and Chemistry of Rare Earths; Gschneider, K. A., Eyring, L., Eds.; Elsevier: Amsterdam, 1984; Chapter 50.
28. See for example: (a) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865. (b) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283 and references therein. (c) Evans, W. J. Adv. Organomet. Chem. 1985, 24, 131 and references therein. (d) Kagan, H. B.; Namy, J. L. In Handbook on the Physics and Chemistry of Rare Earths; Gschneider, K. A., Eyring, L., Eds.; Elsevier: Amsterdam, 1984; Chapter 50.
29. See for example: (a) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865. (b) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283 and references therein. (c) Evans, W. J. Adv. Organomet. Chem. 1985, 24, 131 and references therein. (d) Kagan, H. B.; Namy, J. L. In Handbook on the Physics and Chemistry of Rare Earths; Gschneider, K. A., Eyring, L., Eds.; Elsevier: Amsterdam, 1984; Chapter 50.
30. (a) Dubé, T.; Conoci, S.; Gambarotta, S.; Yap, G. P. A.; Vasapollo, G. Angew. Chem. Int. Ed., in press,
31. (b) Jubb, J.; Gambarotta, S. J. Am. Chem. Soc. 1994, 116, 4477.
32. (a) Piers, W. E.; Shapiro, P. J.; Bunel, E. E.; Bercaw, J. E. Synlett 1990, 74.
33. (b) Qian, C.; Ge, Y.; Deng, D.; Gu, Y.; Zhang, C. J. Organomet. Chem. 1988, 344, 175.
34. (c) Qian, C.; Zhu, D.; Li, D. J. Organomet. Chem. 1992, 430, 175.
35. (d) Piers, W. E.; Bercaw, J. E. J. Am. Chem. Soc. 1990, 112, 9406.
36. Evans, W. J.; Grate, J. W.; Hughes, L. A.; Zhang, H.; Atwood, J. L. J. Am. Chem. Soc. 1985, 107, 3728.
37. (a) Sen, A.; Chebolu, V.; Rheingold, A. L. Inorg. Chem. 1987, 26, 1821.
38. (b) Evans, W. J.; Anwander, R; Ansari, M. A.; Ziller, J. W. Inorg. Chem. 1995, 34, 5.
39. (c) Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Tian, S. J. Chem. Soc., Chem. Commun. 1994, 2691.
40. (d) Biagini, P.; Lugli, G.; Abis, L.; Millini, R. J. Organomet. Chem. 1994, 474, C16.
41. (a) Chebolu, V.; Whittle, R. R.; Sen, A. Inorg. Chem. 1985, 24, 3082.
42. (b) Evans, W. J.; Drummond, D. K.; Zhang, H.; Atwood, J. L. Inorg. Chem. 1988, 27, 575.
43. (c) Evans, W. J.: Rabe, G. W.; Ziller, J. W. Inorg. Chem. 1994, 33, 3072.
44. (d) White, J. P., III; Deng, H.; Boyd, E. P.; Gallucci, J.; Shore, S. G. Inorg. Chem. 1994, 33, 1685.
45. (e) Evans, W. J.; Rabe, G. W.; Ziller, J. W. Organometallics 1994, 13, 1641.
46. (f) Minhas, R.; Song, J.; Ma, Y.; Gambarotta, S. Inorg. Chem. 1996, 35, 1866.
47. (g) Evans, J. W.; Ansari, M. A.; Ziller, J. W. Inorg. Chem. 1996, 35, 5435.
48. (h) Schaverien, C. J.; Orpen, A. G. Inorg. Chem. 1991, 30, 4968.
49. (i) Edelmann, F. T. Coord. Chem. Rev. 1995, 95, 403.
50. (j) Schumann, H.; Rosenthal, E. C. E.; Winterfield, J.; Kociok-Kohn, G. J. Organomet. Chem. 1995, 495, C12.
51. (a) Nief, F.; Ricard, L. J. Organomet. Chem. 1994, 464, 149.
52. (b) Rabe, G.; Riede, J.; Schier, A. Inorg. Chem. 1996, 35, 2680.
53. (c) Gosink, H. J.; Nief, F.; Ricard, L.; Mathey, F. Inorg. Chem. 1995, 34, 1306.
54. (d) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
55. (a) Takats, J. J. Alloys Compd. 1997, 249, 52.
56. (b) Hasinoff, L.; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833.
57. (c) Ferrence, G. M.; McDonald, R.; Takats, J. Angew. Chem., Int. Ed. 1999, 38, 2233.
58. Evans, W. J.; Clark, R. D.; Ansari, M. A.; Ziller, J. W. J. Am. Chem. Soc. 1998, 120, 9555.
59. Song, J.; Gambarotta, S. Angew. Chem., Int. Ed. Engl. 1995, 34, 2141.
60. 3 was prepared and was transformed into the corresponding tetrahydrofuranate by following a standard procedure: (a) Freeman, J. H.; Smith, M. L. J. Inorg. Nucl. Chem. 1958, 7, 224. (b) Manzer, L. E. Inorg. Synth. 1982, 21, 135.
61. 3 was prepared and was transformed into the corresponding tetrahydrofuranate by following a standard procedure: (a) Freeman, J. H.; Smith, M. L. J. Inorg. Nucl. Chem. 1958, 7, 224. (b) Manzer, L. E. Inorg. Synth. 1982, 21, 135.
62. Evans, W. J.; Grate, J. W.; Choi, H. W.; Bloom, I.; Hunter, W. E.; Atwood, J. L. J. Am. Chem. Soc. 1985, 107, 941.
63. Gale, P. A.; Sessler, J. L.; Král, V.; Lynch, V. J. Am. Chem. Soc. 1996, 118, 5140.
64. (a) Mabbs, M. B.; Machin, D. Magnetism and Transition Metal Complexes; Chapman and Hall: London, 1973.
65. (b) Foese, G.; Gorter, C. J.; Smits, L. J. Constantes Selectionnes, Diamagnetisme, Paramagnetisme Relaxation Paramagnetique; Masson: Paris, 1957.
66. Dubé, T.; Gambarotta, S.; Yap, G. P. A. Organometallics, in press.
67. Blessing, R. Acta Crystallogr. 1995, A51, 33-38.
68. Dubé, T.; Gambarotta, S.; Yap, G. P. A. Angew. Chem., Int. Ed. 1998, 38, 1432.
69. Evans, W. J.; Ulibarri, T. A. J. Am. Chem. Soc. 1987, 109, 4292.
70. (a) Knjazhanski, S. Y.; Bulychev, B. M.; Belskii, V. K.; Soloveichik, G. L. J. Organomet. Chem. 1987, 327, 173.
71. (b) Gun'ko, Y. K.; Bulychev, B. M.; Sizov, A. I.; Bel'sky, V. K.; Soloveichik, G. L. J. Organomet. Chem. 1990, 390, 153.
72. (c) Belsky, V. K.; Gun'ko, Y. K.; Bulychev, B. M.; Soloveichik, G. L. J. Organomet. Chem. 1991, 419, 299
73. Belsky, V. K.; Gun'ko, Y. K.; Bulychev, B. M.; Soloveichik, G. L. J. Organomet. Chem. 1991, 420, 43.
74. See for example: (a) Jubb, J.; Gambarotta, S.; Duchateau, R.; Teuben, J. H. J. Chem. Soc., Chem. Commun. 1994, 2641.
75. (b) Aspinall, H. C.; Tillotson, M. R. Inorg. Chem. 1996, 35, 2163.
76. (c) Evans, W. J.; Dominguez, R.; Hanusa, T. P. Organometallics 1986, 5, 1291.
77. (d) Jubb, J.; Gambarotta, S. Inorg. Chem. 1994, 33, 2503.
78. (e) Jubb, J.; Gambarotta, S. J. Am. Chem. Soc. 1993, 115, 10410.
79. (f) Dube, T.; Gambarotta, S.; Yap, G. P. A. Organometallics 1998, 17, 3967.
80. 9a