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21944449789
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Off-axis scans were carried out to determine the rotation relationship in the (022̄3) plane between the selected off-axis 4H reflections: 303̄0 and 033̄0, 101̄2 and 011̄2, and 202̄2 and 022̄2. The calculated angles between the planes based on 4H single crystal (Ref. 6) were 109.6° (or 70.4°), 121° (or 59°), and 97° (or 83°) in that order. These values were compared with the measured ones. This work makes the (022̄3) 4H phase distinguishable from other polymorphs such as 9R or pseudocubic.
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21944437084
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4H reflections were also found to be comparable.
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12
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0001059103
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