First Preparation and X-ray Crystallographic Structure Determination of S,S,S-Triphenylthiazyne

Journal of Organic Chemistry

Volumn 62, Issue 12, 1997, Pages 3802-3803

  Yoshimura, Toshiaki ^a   Hamada, Kohki ^a   Imado, Masahiro ^a   Hamata, Kouki ^a   Tomoda, Kazumi ^a   Fujii, Takayoshi ^a   Morita, Hiroyuki ^a   Shimasaki, Choichiro ^a   Ono, Shin ^a   Tsukurimichi, Eiichi ^a   Furukawa, Naomichi ^b   Kimura, Takeshi ^b  

^a UNIVERSITY OF TOYAMA   (Japan)

^b UNIVERSITY OF TSUKUBA   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000520324     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo9703919     Document Type: Article

References (23)

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2. (b) Glemer, O.; Richert, H.; Anorg, Z. Allg. Chem. 1961, 307, 313.
3. (c) Richert, H.; Glemser, O. Allg. Chem. 1961, 307, 328.
4. (d) Glemser, O.; Meyer, H.; Haas, A. Chem. Ber. 1964, 97, 1704.
5. (d) Glemser, O.; Mews, R. Angew. Chem., Int. Ed. Engl. 1980, 19, 883 and references therein.
6. Clifford, A. F.; Howell, J. L.; Wooton, D. L. J. Fluorine Chem. 1978, 11, 433.
7. (a) Yoshimura, T.; Kita, H.; Takeuchi, K.; Takata, E.; Hasegawa, K.; Shimasaki, C.; Tsukurimichi, E. Chem. Lett. 1992, 1433.
8. (b) Yoshimura, T.; Takata, E.; Miyake, T.; Shimasaki, C.; Hasegawa, K.; Tsukurimichi, E. Chem. Lett. 1992, 2213.
9. (c) Alkoxythiazyne was prepared from S,S-diphenyl-N-halosulfilimine: Yoshimura, T.; Tsukurimichi, E.; Kita, H.; Fujii, H.; Shimasaki, C. Tetrahedron Lett. 1989, 30, 6339.
10. (a) Shaaz, L. J.; Andes, B. A.; Carsky, P.; Zahradnik, R. Inorg. Chem. 1984, 23, 2428.
11. (b) Beach, D. B.; Jolly, W.; Mews, R.; Waterfeld, A. Inorg. Chem. 1984, 23, 4080.
12. 1: C, 73.19; H, 5.80; N, 4.74. Found: C, 73.34; H, 5.69; N, 4.93.
13. Yoshimura, T.; Omata, T,; Furukawa, N.; Oae, S. J. Org. Chem. 1976, 41, 1728.
14. Oae, S.; Harada, K.; Tsujihara, K.; Furukawa, N. Int. J. Sulfur Chem. Part A 1972, 2, 49.
15. 2). The author has deposited atomic coordinates for this structure with the Cambridge Crystallographic Data Centre. The coordinates can be obtained, on request, from the Director, Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK.
16. The S-N bond length of thiazyl trifluoride was determined by microwave spectroscopy. Kirchhoff, W. H.; Wilson, E. B., Jr. J. Am.Chem. Soc. 1962, 84, 334.
17. Kalman, A.; Duffin, B.; Kucsman, A. Acta. Crystallogr., Sect. B 1971, 27, 586.
18. Oberhammer, H.; Zeil, W. Z. Naturforsch., A 1970, 25, 845.
19. Oberhammer, H.; Zeel, W. Z. Naturforsch., A 1969, 24, 1612.
20. 1: C, 68.89; H, 5.14; N, 4.46. Found: C, 68.67; H, 5.02; N, 4.39.
21. Mori, M.; Takeuchi, H.; Minato, H.; Kobayashi, M.; Yoshida, M.; Matsuyama, H.; Kamigata, N. Phosphorus, Sulfur, Silicon 1990, 47, 157.
22. Furukawa, N.; Yoshimura, T.; Omata, T.; Oae, S. Chem. Ind. 1972, A2, 1972.
23. 1: C, 56.38; H, 4.96; N, 3.13. Found: C, 56.35; H, 4.95; N, 3.02.