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Close examination of refs 12 and 30 reveals that there is some confusion over the identity of a single infrared spectrum that was ascribed to both an ammonia-treated sample in one paper and a methylamine-treated sample in the other. Furthermore, in those two papers, there appear to be significant infrared absorptions in the hydroxyl region of both their starting chlorinated diamond species and the product they reported. The authors also cited XPS data, but no spectra are shown and relevant spectroscopic methods information is lacking. Overall, it is not clear that the previous authors' assignment of their product as amine-terminated diamond was well founded.
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D = 1.37. See: Conley, R. T. Infrared Spectroscopy; Allyn and Bacon: Boston, 1966; pp 279-280.
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