Studies of tetrakis(trifluoroacetate) dirhodium Part 4. Solventless synthesis of Rh2(O2CCF3)2CO4 combined with Rh2(O2CCF3)4, a compound with infinite chains of rhodium atoms

Journal of Organometallic Chemistry

Volumn 596, Issue 1-2, 2000, Pages 130-135

  Cotton, F Albert ^a   Dikarev, Evgeny V ^a   Petrukhina, Marina A ^a  

^a TEXAS A AND M UNIVERSITY   (United States)

Author keywords

Carbonyl; Crystal structure; Rhodium; Trifluoroacetate

Indexed keywords

EID: 0000478166     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(99)00609-9     Document Type: Article

References (19)

1. F.A. Cotton, R.A. Walton, Multiple Bonds Between Metal Atoms, 2nd edition, Oxford University Press, New York, 1993.
2. T.R. Felthouse, Progr. Inorg. Chem. 29 (1982) 73.
3. E.B. Boyar, S.D. Robinson, Coord. Chem. Rev. 50 (1983) 109.
4. S.A. Johnson, H.R. Hunt, H.M. Neumann, Inorg. Chem. 2 (1963) 960.
5. F.A. Cotton, E.V. Dikarev, X. Feng, Inorg. Chim. Acta 237 (1995) 19.
6. F.A. Cotton, L.R. Falvello, M. Gerards, G. Snatzke, J. Am. Chem. Soc. 112 (1990) 8979.
7. F.A. Cotton, E.V. Dikarev, unpublished work.
8. F.A. Cotton, E.V. Dikarev, S.-E. Stiriba, Organometallics 18 (1999) 2724.
9. M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, Organometallics 18 (1999) 1747 and references therein.
10. F.A. Cotton, E.V. Dikarev, S.-E. Stiriba, Inorg. Chem. 38 (1999) 4877.
11. J. Pflugrath, A. Messerschmitt, MADNES, Munich Area Detector (New EEC) System, version EEC 11/9/89, with enhancements by Enraf-Nonius Corp., Delft, The Netherlands. A description of MADNES appears in: A. Messerschmitt, J. Pflugrath, J. Appl. Crystallogr. 20 (1987) 306.
12. (a) W. Kabsch, J. Appl. Crystallogr. 21 (1988) 67.
13. (b) W. Kabsch, J. Appl. Crystallogr. 21 (1988) 916.
14. SHELXTL V.5, Siemens Industrial Automation Inc., Madison, WI, 1994.
15. G.M. Sheldrick, in: H.D. Flack, L. Parkanyi, K. Simon (Eds.), Crystallographic Computing 6, Oxford University Press, Oxford, 1993, p. 111.
16. x has appeared. See: M.E. Prater, L.E. Pence, R. Clérac, G.M. Finniss, C. Campana, P. Auban-Senzier, D. Jérome, E. Canadell, K.R. Dunbar, J. Am. Chem. Soc. 121 (1999) 8005.
17. 3) have been mentioned as intermediates in the synthesis of other rhodium compounds. See: F.J. Lahoz, A. Martin, M.A. Esteruelas, E. Sola, J.L. Serrano, L.A. Oro, Organometallics, 10 (1991) 1794.
18. J.G. Bullitt, F.A. Cotton, Inorg. Chim. Acta 5 (1971) 406.
19. See: J.S. Miller (Ed.), Extended Linear Chain Compounds, vols. 1-3, Plenum Press, New York, 1982.