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33745385982
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note
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3, Z = 8, T = 210 K, ⊙ region 2.9° ≤ 2 ⊙ ≤
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20
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33745355965
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note
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2 refinement). All data sets were collected on a Siemens-Nicolet R3m/V diflractometer. Mo-Kα radiation (X, = 71.07 pm), graphite monochromator, solution and refinement: SHELXL93 P' and SHELXTL Plus [10). Atomic coordinates, bond lengths and angles, and thermal parameters of 3 have been deposited at the Cambridge Crystallographic Data Centre; requests for data should be accompanied by declaration of the reference code NABGOM. Full tables of positional and thermal parameters of 4, including those of counterions and solvate molecules, and of the structure factor amplitudes are available as supplementary material at the Fachinformationszentrum Karlsruhe, Gesellschaft für wissenschaftlich-technische Information mbH, D-76344 EggensteinLeopoldshafen, by declaration of the CSD-406450 the author names and the quotation.
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