A Thermometer for Nonspinning Solid-State NMR Spectroscopy

Journal of Magnetic Resonance

Volumn 146, Issue 2, 2000, Pages 379-380

  Beckmann, Peter A ^a,b   Dybowski, Cecil ^a  

^a UNIVERSITY OF DELAWARE   (United States)

^b BRYN MAWR COLLEGE   (United States)

Author keywords

207 Pb; Calibration; Chemical shift; Lead nitrate; Temperature

Indexed keywords

EID: 0000365067     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2000.2171     Document Type: Editorial

References (6)

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3. 13 C chemical shifts which obey the Curie law in CP/MAS spectra. The first CP/MAS chemical shift thermometer, J. Magn. Reson. 69, 191-195 (1986).
4. 207 Pb MAS spectra of solid lead nitrate. An accurate, sensitive thermometer for variable temperature MAS, J. Magn. Reson. A 116, 215-220 (1995).
5. 2+ chemical shift tensors from precise powder lineshape analysis, Solid State Nucl. Magn. Reson. 6, 241-250 (1996).
6. G. Neue and C. Dybowski, Determining temperature in a magic-angle spinning probe using the temperature dependence of the isotropic chemical shift of lead nitrate, Solid State Nucl. Magn. Reson. 7, 333-336 (1997).