Stable rac-[1,2-ethylene-1,1′-bis(η 5-tetrahydroindenyl)]-zirconacyclopentanes. Syntheses, X-ray crystal structures, stability, and catalysis of ethylene polymerization

Organometallics

Volumn 16, Issue 13, 1997, Pages 2886-2890

  Mansel, Stefan ^a   Thomas, Dominique ^a   Lefeber, Claudia ^a   Heller, Detlef ^a   Kempe, Rhett ^a   Baumann, Wolfgang ^a   Rosenthal, Uwe ^a  

^a UNIVERSITY OF ROSTOCK   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000340942     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om9700324     Document Type: Article

References (27)

1. For reviews, see: (a) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047. (b) Buchwald, S. L.; Fisher, R. A. Chem. Scr. 1989, 29, 417. (c) Negishi, E. Chem. Scr. 1989, 29, 457. (d) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124. (e) Negishi, E.; Maye, J. P.; Choueiry, D. Tetrahedron 1995, 51, 4447.
2. For reviews, see: (a) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047. (b) Buchwald, S. L.; Fisher, R. A. Chem. Scr. 1989, 29, 417. (c) Negishi, E. Chem. Scr. 1989, 29, 457. (d) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124. (e) Negishi, E.; Maye, J. P.; Choueiry, D. Tetrahedron 1995, 51, 4447.
3. For reviews, see: (a) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047. (b) Buchwald, S. L.; Fisher, R. A. Chem. Scr. 1989, 29, 417. (c) Negishi, E. Chem. Scr. 1989, 29, 457. (d) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124. (e) Negishi, E.; Maye, J. P.; Choueiry, D. Tetrahedron 1995, 51, 4447.
4. For reviews, see: (a) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047. (b) Buchwald, S. L.; Fisher, R. A. Chem. Scr. 1989, 29, 417. (c) Negishi, E. Chem. Scr. 1989, 29, 457. (d) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124. (e) Negishi, E.; Maye, J. P.; Choueiry, D. Tetrahedron 1995, 51, 4447.
5. For reviews, see: (a) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047. (b) Buchwald, S. L.; Fisher, R. A. Chem. Scr. 1989, 29, 417. (c) Negishi, E. Chem. Scr. 1989, 29, 457. (d) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124. (e) Negishi, E.; Maye, J. P.; Choueiry, D. Tetrahedron 1995, 51, 4447.
6. (a) Erker, G.; Zwettler, R.; Krüger, C.; Hyla-Kryspin, I.; Gleiter, R. Organometallics 1990, 9, 524.
7. (b) Takahashi, T.; Fischer, R.; Xi, Z.; Nakajima, K. Chemistry Lett. 1996, 357.
8. (c) Podubrin, S. Ph.D. Thesis, University of Kaiserslautern, 1993,
9. Xi, Z.; Hara, R.; Takahashi, T. J. Org. Chem. 1995, 60, 4444.
10. Dorf, U.; Engel, K.; Erker, G. Angew. Chem. 1982, 94, 916.
11. Knight, K. S.; Wang, D.; Waymouth, R. M.; Ziller, J. J. Am. Chem. Soc. 1994, 116, 1845.
12. Lefeber, C.; Baumann, W.; Tillack, A.; Kempe, R.; Görls, H.; Rosenthal, U. Organometallics 1996, 15, 3486.
13. Heller, D.; Baumann, W.; Mansel, S. Magn. Reson. Chem., in press.
14. 8.
15. Rosenthal, U.; Ohff, A.; Michalik, M.; Görls, H.; Burlakov, V. .; Shur; B. B. Angew. Chem. 1993, 105, 1228.
16. Negishi, E.; Choueiry, D.; Nguyen, T.; Swanson, D. J. Am. Chem. Soc. 1994, 116, 9751.
17. Swanson, D.; Rousset, C.; Negishi, E. J. Org. Chem. 1989, 54, 3521
18. Takahashi, T.; Suzuki, N.; Hasegawa, M.; Nitto, Y.; Aoyagi, K.; Saburi, M. Chemistry Lett. 1992, 331.
19. Böhme, U.; Thiele, K.-H.; Rufinska, A. Z. Anorg. Allg. Chem. 1994, 620, 1455.
20. (a) Erker, G.; Dorf, U.; Rheingold, A. L. Organometallics 1988, 7, 138.
21. (b) Erker, G.; Zwettler, R. J. Organomet. Chem. 1991, 409, 179.
22. (c) Hara, R.; Xi, Z.; Kotora, M.; Xi, C.; Takahashi, T. Chem. Lett. 1996, 1003.
23. Grubbs, R. H.; Miyashita, A. J. Am. Chem. Soc. 1978, 100, 1300.
24. Baumann, W.; Ohff, A.; Ebener, M. Helv. Chim. Acta 1996, 79, 454.
25. Ohff, A.; Pulst, S.; Lefeber, C.; Peulecke, N.; Arndt, F.; Burlakov, V. V.; Rosenthal, U. Synlett 1996, 111.
26. SHELXS-86, Sheldrick, G. M. Acta Crystallogr. 1990, A46, 467.
27. Sheldrick, G. M. SHELXL-93, University of Göttingen, Göttingen, Germany, 1993.