Neutral PtRh2 and PtRh4 tetraalkynyl complexes. X-ray crystal structures of {Pt(C=CBut)4[Rh2(μ-X)(COD)2] 2} (X = Cl, OH)

Organometallics

Volumn 16, Issue 18, 1997, Pages 3921-3926

  Ara, Irene ^a   Berenguer, Jesús R ^b   Forniés, Juan ^a   Lalinde, Elena ^b  

^a UNIVERSITY OF ZARAGOZA   (Spain)

^b UNIVERSITY OF LA RIOJA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000335586     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om9702587     Document Type: Article

References (48)

1. (a) Nast, R. Coord. Chem. Rev. 1982, 47, 89.
2. (b) Bruce, M. I. Chem. Rev. 1983, 83, 203.
3. (c) Akita, M.; Moro-Oka, Y. Bull. Chem. Soc. Jpn. 1995, 68, 420.
4. (d) Manna, J.; Jonh, K. D.; Hopkins, M. D. Adv. Organomet. Chem. 1996, 79.
5. (a) Beck, W.; Niemer, B.; Wieser, M. Angew. Chem., Int. Ed. Engl. 1993, 32, 923.
6. (b) Lotz, S.; Van Rooyen, P. H.; Meyer, R. Adv. Organomet. Chem. 1995, 37, 219.
7. (c) Lang, H.; Köhler, K.; Blau, S. Coord. Chem. Rev. 1995, 143, 113.
8. (d) Pavan Kumar, P. N. V.; Jemmins, D. J. Am. Chem. Soc. 1988, 110, 125.
9. (e) Rosenthal, U.; Pulst, S.; Arndt, P.; Ohff, A.; Tillack, A.; Baumann, W.; Kempe, R.; Burlakov, V. V. Organometallics 1995, 14, 2961.
10. (f) Varga, V.; Mach, K.; Hiller, J.; Thewalt, U.; Sedmera, P.; Polásek, M. Organometallics 1995, 14, 1410.
11. (g) Erker, G.; Albrecht, M.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
12. (h) Lee, L.; Berg, D. J.; Bushnell, G. W. Organometallics 1995, 14, 5021.
13. (i) Chang, C. C.; Srinivas, B.; Wu, M. L.; Chiang, W. H.; Chiang, M. Y.; Hsiung, C. S. Organometallics 1995, 14, 5150.
14. (j) Janssen, M. D.; Köhler, K.; Herres, M.; Dedin, A.; Smeets, W. J. J.; Spek, A. L.; Grove, D. M.; Lang, H.; van Koten, G. J. Am. Chem. Soc. 1996, 118, 4817.
15. (k) Forniés, J.; Lalinde, E. J. Chem. Soc., Dalton Trans. 1996, 2587 (Perspective).
16. (a) Boncella, J. M.; Tilley, T. D.; Andersen, R. A. J. Chem. Soc., Chem. Commun. 1984, 710.
17. (b) Yamazaki, S.; Deeming, A. J. J. Chem. Soc., Dalton Trans. 1993, 3051.
18. (c) Edwards, A. J.; Fallaize, A.; Raithby, P. R.; Rennie, M. A.; Steiner, A.; Verhovevoort, K. L.; Wright, D. S. J. Chem. Soc., Dalton Trans. 1996, 133.
19. (d) Kawaguchi, H.; Tatsumi, K, Organometallics 1995, 14, 4294.
20. (a) Forniés, J.; Lalinde, E.; Martín, A.; Moreno, M. T. J. Chem. Soc., Dalton Trans. 1994, 135.
21. (b) Berenguer, J. R.; Forniés, J.; Lalinde, E.; Martin, A.; Moreno, M, T. J. Chem. Soc., Dalton Trans. 1994, 3343.
22. (c) Forniés, J.; Lalinde, E.; Martin, A.; Moreno, M. T. J. Organomet. Chem. 1995, 490, 179.
23. (a) Forniés, J.; Gómez-Saso, M. A.; Lalinde, E.; Martínez, F.; Moreno, M. T. Organometallics 1992, 11, 2873.
24. (b) Berenguer, J. R.; Forniés, J.; Lalinde, E.; Martinez, F. J. Organomet. Chem. 1994, 470, C15.
25. (c) Berenguer, J. R.; Forniés, J.; Lalinde, E.; Martínez, F. J. Chem. Soc., Chem. Commun. 1995, 1227.
26. (d) Berenguer, J. R.; Forniés, J.; Lalinde, E.; Martinez, F. Organometallics 1996, 15, 4537.
27. (a) Erker, G.; Frömberg, W.; Benn, R.; Mynott, R.; Angermund, K.; Krüger, C. Organometallics 1989, 8, 911.
28. (b) Lang, H.; Blau, S.; Nuber, B.; Zsolnai, L. Organometallics 1995, 14, 3216 and references given therein,
29. (c) Lang, H.; Blau, S.; Pritzkow, H.; Zsolnai, L. Organometallics 1995, 14, 1850.
30. Preparation: (a) Usón, R.; Oro, L. A.; Cabeza, J. A. Inorg. Synth. 1985, 23, 126. X-ray structure: (b) Selent, D.; Ramm, M. J. Organomet. Chem. 1995, 485, 135. (c) Brune, H.-A.; Hemmer, R.; Unsin, J.; Holl, K.; Thewalt, Z. Z. Naturforsch. 1988, 43B, 487. (d) Gevert, O.; Wolf, J.; Werner, H. Organometallics 1996, 15, 2806.
31. Preparation: (a) Usón, R.; Oro, L. A.; Cabeza, J. A. Inorg. Synth. 1985, 23, 126. X-ray structure: (b) Selent, D.; Ramm, M. J. Organomet. Chem. 1995, 485, 135. (c) Brune, H.-A.; Hemmer, R.; Unsin, J.; Holl, K.; Thewalt, Z. Z. Naturforsch. 1988, 43B, 487. (d) Gevert, O.; Wolf, J.; Werner, H. Organometallics 1996, 15, 2806.
32. Preparation: (a) Usón, R.; Oro, L. A.; Cabeza, J. A. Inorg. Synth. 1985, 23, 126. X-ray structure: (b) Selent, D.; Ramm, M. J. Organomet. Chem. 1995, 485, 135. (c) Brune, H.-A.; Hemmer, R.; Unsin, J.; Holl, K.; Thewalt, Z. Z. Naturforsch. 1988, 43B, 487. (d) Gevert, O.; Wolf, J.; Werner, H. Organometallics 1996, 15, 2806.
33. Preparation: (a) Usón, R.; Oro, L. A.; Cabeza, J. A. Inorg. Synth. 1985, 23, 126. X-ray structure: (b) Selent, D.; Ramm, M. J. Organomet. Chem. 1995, 485, 135. (c) Brune, H.-A.; Hemmer, R.; Unsin, J.; Holl, K.; Thewalt, Z. Z. Naturforsch. 1988, 43B, 487. (d) Gevert, O.; Wolf, J.; Werner, H. Organometallics 1996, 15, 2806.
34. Preparation: (a) Chatt, J.; Venanzi, L. M. J. Chem. Soc. 1957, 4735. (b) Giordano, G.; Crabtree, R. H. Inorg. Synth. 1990, 28, 88. X-ray structure: (c) Ibers, J. A.; Snyder, R. G. Acta Crystallogr. 1962, 15, 923. (d) Curtis, M. D.; Butler, W. M.; Greene, J. Inorg. Chem. 1978, 17, 2928. (e) Binger, P.; Haas, J.; Glaser, G.; Goddard, R.; Krüger, C. Chem. Ber. 1994, 727, 1927.
35. Preparation: (a) Chatt, J.; Venanzi, L. M. J. Chem. Soc. 1957, 4735. (b) Giordano, G.; Crabtree, R. H. Inorg. Synth. 1990, 28, 88. X-ray structure: (c) Ibers, J. A.; Snyder, R. G. Acta Crystallogr. 1962, 15, 923. (d) Curtis, M. D.; Butler, W. M.; Greene, J. Inorg. Chem. 1978, 17, 2928. (e) Binger, P.; Haas, J.; Glaser, G.; Goddard, R.; Krüger, C. Chem. Ber. 1994, 727, 1927.
36. Preparation: (a) Chatt, J.; Venanzi, L. M. J. Chem. Soc. 1957, 4735. (b) Giordano, G.; Crabtree, R. H. Inorg. Synth. 1990, 28, 88. X-ray structure: (c) Ibers, J. A.; Snyder, R. G. Acta Crystallogr. 1962, 15, 923. (d) Curtis, M. D.; Butler, W. M.; Greene, J. Inorg. Chem. 1978, 17, 2928. (e) Binger, P.; Haas, J.; Glaser, G.; Goddard, R.; Krüger, C. Chem. Ber. 1994, 727, 1927.
37. Preparation: (a) Chatt, J.; Venanzi, L. M. J. Chem. Soc. 1957, 4735. (b) Giordano, G.; Crabtree, R. H. Inorg. Synth. 1990, 28, 88. X-ray structure: (c) Ibers, J. A.; Snyder, R. G. Acta Crystallogr. 1962, 15, 923. (d) Curtis, M. D.; Butler, W. M.; Greene, J. Inorg. Chem. 1978, 17, 2928. (e) Binger, P.; Haas, J.; Glaser, G.; Goddard, R.; Krüger, C. Chem. Ber. 1994, 727, 1927.
38. Preparation: (a) Chatt, J.; Venanzi, L. M. J. Chem. Soc. 1957, 4735. (b) Giordano, G.; Crabtree, R. H. Inorg. Synth. 1990, 28, 88. X-ray structure: (c) Ibers, J. A.; Snyder, R. G. Acta Crystallogr. 1962, 15, 923. (d) Curtis, M. D.; Butler, W. M.; Greene, J. Inorg. Chem. 1978, 17, 2928. (e) Binger, P.; Haas, J.; Glaser, G.; Goddard, R.; Krüger, C. Chem. Ber. 1994, 727, 1927.
39. (a) Hutton, A. T.; Shebanzadeh, B.; Shaw, B. L. J. Chem. Soc., Chem. Commun. 1984, 549.
40. (b) Cowie, M.; Loeb, S. Organometallics 1985, 4, 852.
41. (c) Esteruelas, M. A.; Lahuerta, O.; Modrego, J.; Nürnberg, O.; Oro, L. A.; Rodríguez, L.; Sola, E.; Werner, H. Organometallics 1993, 12, 266.
42. (d) Antwi-Nsiah, H. F.; Oke, O.; Cowie, M. Organometallics 1996, 15, 506.
43. Within the +15 to -50 °C range the olefinic resonances practically do not merge from the base line.
44. Ara, I.; Berenguer, J. R.; Fornies, J.; Lalinde E.; Martínez, F. XV Meeting of the Spanish Organometallic Chemistry Group, Sevilla, 1995.
45. Ara, I.; Berenguer, J. R.; Eguizábal, E.; Lalinde, E.; Forniés, J. Unpublished results.
46. Espinet, P.; Forniés, J.; Martínez, F.; Tomás, M.; Lalinde, E.; Moreno, M. T.; Ruiz, A.; Welch, A. J. J. Chem. Soc., Dalton Trans. 1990, 791.
47. SHELXTL-PLUS, Software Package for the Determination of Crystal Structures, Release 4.0; Siemens Analytical X-ray Instruments, Inc., Madison, WI, 1990.
48. Sheldrick, G. M. SHELXL-93: FORTRAN Program for The Refinement of Crystal Structures from Diffraction Data; University of Göttingen, Göttingen, Germany, 1993.