False AA′X spin-spin coupling systems in 13C NMR: examples involving phosphorus and a 20-year-old mystery in off-resonance decoupling

Journal of Chemical Education

Volumn 74, Issue 12, 1997, Pages 1485-1489

  Hersh, William H ^a  

^a CITY UNIVERSITY OF NEW YORK   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000314595     PISSN: 00219584     EISSN: None     Source Type: Journal    
DOI: 10.1021/ed074p1485     Document Type: Article

References (19)

1. Wehrli, F. W.; Wirthlin, T. Interpretation of Carbon-13 NMR Spectra; Heyden: London, 1978; pp 72-76.
2. Andrews, G. T.; Colquhoun, I. J.; McFarlane, W. Polyhedron 1983, 2, 783-790.
3. Redfield, D. A.; Nelson, J. H.; Cary, L. W. Inorg. Nucl. Chem. Lett. 1974, 10, 727-733.
4. Redfield, D. A.; Cary, L. W.; Nelson, J. H. Inorg. Chem. 1975, 14, 50-59.
5. Friebolin, H. Basic One- and Two-Dimensional NMR Spectroscopy; 2nd ed.; VCH; New York, 1993; p 124.
6. Verstuyft, A. W.; Nelson, J. H.; Cary, L. W. Inorg. Chem. 1976, 15, 732-734.
7. King, R. B.; Cloyd, J. C. J. J. Chem. Soc., Perkin Trans. 2 1975, 938-941.
8. 13C NMR of Transition Metal Phosphine Complexes, Vol. 16; Springer; Berlin, 1979.
9. Musher, J. I.; Corey, E. J. Tetrahedron 1962, 18, 791-809.
10. Hersh, W. H.; Xu, P.; Wang, B.; Yom, J. W.; Simpson, C. K. Inorg. Chem. 1996, 35, 5453-5459.
11. Pregosin, P. S.; Kunz, R. Helv. Chim. Acta 1975, 58, 423-431.
12. Jolly, P. W.; Mynott, R. In Advances in Organometallic Chemistry, Vol. 19; Stone, F. G. A.; West, R., Eds.; Academic: San Diego, 1981; pp 257-304.
13. Andrews, M. A.; Voss, E. J.; Gould, G. L.; Klooster, W. T.; Koetzle, T. F. J. Am. Chem. Soc. 1994, 116, 5741-5746.
14. Harris, R. K.; Jones, M. S.; Kenwright, A. M. Magn. Reson. Chem. 1993, 31, 1085-1087.
15. Kimpton, B. R.; Mcfarlane, W.; Muir, A. S.; Patel, P. G.; Bookham, J. L. Polyhedron 1993, 12, 2525-2534.
16. Fritz, H.; Sauter, H. J. Magn. Reson. 1974, 15, 177-180.
17. Newmark, R. A.; Hill, J. R. J. Am. Chem. Soc. 1973, 95, 4435-4437.
18. Fritz, H.; Sauter, H. J. Magn. Reson. 1975, 18, 527-544.
19. MacDonald, J. C.; Mazurek, M. J. Magn. Reson. 1975, 19, 51-57.