Structure-Spectroscopy Correlations in Silver Thiolates: Application to the Structure of Silver 1,5-Pentanedithiolate

Inorganic Chemistry

Volumn 36, Issue 23, 1997, Pages 5299-5305

  Fijolek, Hilary G ^a   González Duarte, Pilar ^c   Park, Sang Hyun ^b   Suib, Steven L ^b   Natan, Michael J ^a  

^a PENNSYLVANIA STATE UNIVERSITY   (United States)

^b UNIVERSITY OF CONNECTICUT   (United States)

^c UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000301613     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9608307     Document Type: Article

References (71)

1. Dance, I. G.; Fisher, K. J.; Banda, R. M. H.; Scudder, M. L. Inorg. Chem. 1991, 30, 183.
2. Baena, M. J.; Espinet, P.; Lequerica, M. C.; Levelut, A. M. J. Am. Chem. Soc. 1992, 114, 4182.
3. (a) Block, E.; Gernon, M.; Kang, H.; Ofori-Okai; G.; Zubieta, J. Inorg. Chem. 1989, 28, 1263.
4. (h) Block, E.; Macherone, D.; Shaikh, S. N.; Zuhieta, J. Polyhedron 1990, 9, 1429.
5. (c) Dance, I. G. Aust. J. Chem. 1978, 31, 2195.
6. (d) Dance, I. G. Inorg. Chim. Acta 1977, 25, L17.
7. (e) Dance. I. G. Inorg. Chem. 1981, 20, 1487.
8. (f) Casals, I.; GonzálezDuarte, P.; Sola, J.; Vives, J.; Font-Bardia, M.; Solans, X. Polyhedron 1990, 9, 769.
9. (a) Dance, I. G.; Fitzpatrick, L. J.; Craig, D. C.; Scudder, M. L. Inorg. Chem. 1989, 28, 1853.
10. (b) Tang, K.; Aslam, M.; Block, E.; Nicholson, T.; Zubieta, J. Inorg. Chem. 1987, 26, 1488.
11. (c) Tang, K.; Yang, J.; Yang, Q.; Tang, Y. J. Chem. Soc., Dalton Trans. 1989, 2297.
12. (d) Henkel, G.; Betz, P.; Krebs, B. Angew. Chem. Int. Ed. Engl. 1987, 26, 145.
13. (e) Henkel, G.; Krebs, B.; Betz, P.; Fietz, H.; Saatkamp, K. Angew. Chem., Int. Ed. Engl. 1988, 27, 1326.
14. (a) Giroud-Godquin, A.-M.; Maitlis. P. M. Angew. Chem., Int. Ed. Engl. 1991, 30, 375.
15. (b) Hudson, S. A.; Maitlis, P. M. Chem. Rev. 1993, 93, 861.
16. (a) Åkerstrom, S. Ark. Kemi 1965, 24, 505.
17. (b) Hong, S. H.; Olin, Å.; Hesse, R. Acta Chem. Scand. 1975, A29, 583.
18. (c) Dance, I. G. Polyhedron 1986, 5, 1037.
19. Dance, I. G.; Fitzpatrick, L. J.; Rae, A. D.; Scudder, M. L. Inorg. Chem. 1983, 22, 3785.
20. (a) Ulman, A. An Introduction to Ultrathin Organic Films: From Langmuir-Blodgett to Self-Assembly; Academic Press, Inc: Boston. 1991.
21. (b) Bain, C. D.; Whitesides, G. M. Angew. Chem., Int. Ed. Engl. 1989, 28, 506.
22. (c) Dubois, L. H.; Nuzzo, R. G. Annu. Rev. Phys. Chem. 1992, 43, 437.
23. (a) Walczak, M. M.; Chung, C.; Stole, S. M.; Widrig, C. A.; Porter, M. D. J. Am. Chem. Soc. 1991, 113, 2370.
24. (b) Fenter, P., Eisenberger, P.; Li, J.; Camillone, N., III; Bernasek, S.; Scoles, G.; Ramanarayanan, T. A.; Liang, K. S. Langmuir 1991, 7, 2013.
25. (c) Laibinis, P. E.; Fox, M. A.; Folkers, J. P.; Whitesides, G. M. Langmuir 1991, 7, 3167.
26. (d) Laibinis, P. E.; Whitesides, G. M.; Allara, D. L.; Tao, Y.-T.; Parikh, A. N.; Nuzzo, R. G. J. Am Chem. Soc. 1991, 113, 7152.
27. (e) Sellers, H.; Ulman, A.; Shnidman, Y.; Eilers, J. E. J. Am. Chem. Soc. 1993, 115, 9389.
28. 109Ag NMR, diffuse reflectance UV-vis, and Raman data for T and G can be found in the following: Fijolek, H. G.; Grohal, J. R.; Sample, J. L.; Natan, M. J. Inorg. Chem. 1997, 36, 622.
29. (a) Zelazowski, A. J.; Stillman, M. J. Inorg. Chem. 1992, 31, 3363.
30. (b) Zelazowski, A. J.; Gasyna, Z.; Stillman, M. J. J. Biol. Chem. 1989, 264, 17091.
31. (c) Casas-Finet, J. R.; Hu, S.; Hamer, D.; Karpel, R. L. Biochemistry 1992, 31, 6617.
32. (d) Grill, E.; Winnacker, E-L.; Zenk, M. H. Proc. Natl. Acad. Sci. U.S.A. 1987, 84, 439.
33. (e) Narula, S. S.; Mehra, R. K.; Winge, D. R.; Armitage, I. M. J. Am. Chem. Soc. 1991, 113, 9354.
34. (f) Narula, S. S.; Winge, D. R.; Armitage, I. M. Biochemistry 1993, 32, 6773.
35. Fijolek, H. G.; Oriskovich, T. O.; Benesi, A. J.; Gonzáles-Duarte, P.; Natan, M. J. Inorg. Chem. 1996, 35, 797.
36. (a) Boroumand, F.; Moser, J.; van den Bergh, H. Appl. Sprectrose 1992, 46, 1874.
37. (b) Hembree, D. M., Jr.; Smyrl, H. R. Appl. Spectrose 1989, 43, 267.
38. (a) Canty, A. J.; Kishimoto, R.; Deacon, G. B.; Farqaharson, G. J. Inorg. Chim. Acta 1976, 20, 161.
39. (b) Canty, A. J.; Kishimoto, R. Inorg. Chim. Acta 1977, 24, 109.
40. González-Duarte, P.; Sola, J.; Vives, J.; Solans, X. J. Chem. Soc. Chem. Commun. 1987, 1641.
41. Wright, J. G.; Natan, M. J.; MacDonnell, F. M.; Ralaton, D. M. O'Halloran, T. V. Prog. Inorg. Chem. 1990, 38, 323 and references therein.
42. Fijolek, H. G.; Natan, M. J. Unpublished observations.
43. The spinning side bands give a measure of the chemical shift anisotropy, which for 1 and 3 at room temperature is equivalent to that of most flexible organic compounds at 77 K or below. For example, see: Duncan, T. M. A Compilation of Chemical Shift Anisotropies; Farragut Press: Madison, WI, 1990.
44. Fyfe, C. A. Solid State NMR for Chemists; CRC Press: Guelph, Ontario, 1983; Chapter 5.
45. Merwin, L. H.; Sebald, A. J. Magn. Reson. 1992, 97, 628.
46. Dollish, F. R.; Fateley, W. G.; Bentley, F, F. Characteristic Roman Frequencies of Organic Compounds; John Wiley and Sons: New York. 1974; Chapter 5 and references therein.
47. (a) Bryant, M. A.; Pemberton, J. E. J. Am. Chem. Soc. 1991, 113, 3629.
48. (b) Bryant, M. A.; Pemberton, J. E. J. Am. Chem. Soc. 1991, 113, 8284.
49. (c) Joo, T. H.; Kim, K.; Kim, M. S. J. Mol Struct. 1987, 158, 265.
50. (d) Nandy, S. K.; Mukherjee, D. K. Indian J. Phys. 1974, 48, 81.
51. (e) Sobocinski, R. L.; Bryant, M. A.; Pemberton, J. E. J. Am. Chem. Soc. 1990, 112, 6177.
52. (f) Pemberton, J. E.; Bryant, M. A.; Sobocinski, R. L.; Joa, S. L. J. Phys. Chem. 1992, 96, 3776.
53. (g) Sandroff, C. J.; Garoff, S.; Leung, K. P. Chem. Phys. Lett. 1983, 96,
54. (a) Joo, T. H.; Kim, K.; Kim, M. S. J. Phys. Chem. 1986, 90, 5816.
55. (b) Joo, T. H.; Kim, M. S.; Kim, K. J. Mol. Struct. 1987, 160, 81.
56. (c) Watanabe, T.; Maeda, H. J. Phys. Chem. 1989, 93, 3258.
57. (d) Kwon, C. K.; Kim, M. S.; Kim, K. J. Mol. Struct. 1987, 162, 201.
58. (e) Kwon. C. K.; Kim, M. S.; Kim, K. J. Raman Spectrosc. 1989, 20, 575.
59. (f) Lee, S. B.; Kim, K.; Kim, M. S.; Oh, W. S.; Lee, Y. S. J. Mol. Struct. 1993, 296, 5.
60. (a) Memon, A.; Khan, M. N.; Al-Dallal, S.; Tanner, D. B.; Porter, C. D. Int. J. Mod. Phys. 1990, 4, 1889.
61. (b) Holmes, P. D.; McDougall. G. S. Wilcock, L. C.; Waugh, K. C. Catal. Today 1991, 9, 15.
62. Pennington, R. E.; Scott, D. W.; Finke, H. L.; McCullough, J. P.; Messerly, J. F.; Hossenlopp, I. A.; Waddington, G. J. Am Chem. Soc. 1956, 78, 3266.
63. Hayashi, M.; Shiro, Y.; Murata, H.; Oshima, T. Bull. Chem. Soc. Jpn. 1965, 38, 1734.
64. Reference 21d.
65. Bowmaker, G. A.; Tan, L.-C. Aust. J. Chem. 1979, 32, 1443.
66. Bowmaker, G. A. In Spectroscopy of Inorganic-Based Materials; Clark. R. J. H., Hester, R. E., Eds; John Wiley & Sons: New York. 1987; pp 1-117.
67. Bowmaker, G. A.; Rogers, D. A. J. Chem. Soc., Dalton Trans. 1982, 1873.
68. Chadha, R. K.; Kumar, R.; Tuck, D. G. Can. J. Chem. 1987, 65, 1336.
69. Matthews, F. W.; Warren, G. G.; Mitchell, J. H. Anal. Chem. 1959, 22, 514.
70. 17
71. Note that, by symmetry, 1 has two C(1)-C(2) bonds; it is not possible to tell whether the gauche interactions appear individually or in pains.