Single-Pulse MAS, Selective Hahn Echo MAS, and 3QMAS NMR Studies of the Mineral Zoisite at 400, 500, 600, and 800 MHz. Exploring the Limits of Al NMR Detectability

Journal of Physical Chemistry B

Volumn 104, Issue 49, 2000, Pages 11612-11616

  Alemany, Lawrence B ^a   Callender, Rhonda L ^a   Barron, Andrew R ^a   Steuernagel, Stefan ^b   Iuga, Dinu ^c   Kentgens, Arno P M ^c  

^a RICE UNIVERSITY   (United States)

^b Bruker Analytik GmbH   (Germany)

^c RADBOUD UNIVERSITY NIJMEGEN   (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000291671     PISSN: 15206106     EISSN: None     Source Type: Journal    
DOI: 10.1021/jp002066m     Document Type: Article

References (32)

1. Bryant, P. L.; Harwell, C. R.; Wu, K.; Fronczek, F. R.; Hall, R. W.; Butler, L. G. J. Phys. Chem. A 1999, 103, 5246.
2. Alemany, L. B.; Steuernagel, S.; Amoureux, J.-P.; Callender, R. L.; Barron, A. R. Solid State Nucl. Magn. Reson. 1999, 14, 1.
3. Kentgens, A. P. M.; Verhagen, R. Chem. Phys. Lett. 1999, 300, 435.
4. Madhu, P. K.; Goldbourt, A.; Frydman, L.; Vega, S. Chem. Phys. Lett. 1999, 307, 41.
5. (a) Goldbourt, A.; Madhu, P. K.; Frydman, L.; Vega. S. "Fast rf Amplitude Modulation in MQMAS NMR Spectroscopy," oral presentation, 41st Rocky Mountain Conference, Denver, August 1999.
6. (b) Vega, S. "Modulated Irradiation Fields in Solid State NMR," oral presentation T18, 1st Alpine Conference on Solid-State NMR, Chamonix, France, September 1999.
7. Iuga, D.; Kentgens, A. P. M. "Double Frequency Sweeps in Static, MAS, and MQMAS NMR," oral presentation T5, 1st Alpine Conference on Solid-State NMR, Chamonix, France, September 1999.
8. Vosegaard, T.; Florian, P.; Grandinetti, P. J.; Massiot. D. "Pure Absorption Mode Spectra Using Modulated RF MQMAS Experiments," poster presentation P96, 1st Alpine Conference on Solid-State NMR, Chamonix, France, September 1999.
9. Engelhardt, G.; Kentgens. A. P. M.; Koller, H.; Samoson, A. Solid State Nucl. Magn. Reson. 1999, 15, 171.
10. Madhu, P. K.; Goldbourt, A.; Frydman, L.; Vega, S. J. Chem. Phys. 2000, 112, 2377.
11. Vosegaard, T.; Florian, P.; Grandinetti, P. J.; Massiot, D. J. Magn. Reson. 2000, 143, 217.
12. Fernandez, C.; Montouillout, V. "Optimization of 3/2 and 5/2 MQMAS using variable amplitude modulation: Numerical and experimental results," poster M/T PH 308, Experimental Nuclear Magnetic Resonance Conference, Pacific Grove CA, April 2000.
13. Goldbourt, A.; Madhu, P. K.; Vega, S. Chem. Phys. Lett. 2000, 320, 448.
14. Iuga, D.; Schäfer, H.; Verhagen, R.; Kentgens, A. P. M. J. Magn. Reson., in press.
15. Vosegaard, T.; Massiot, D.; Grandinetti, P. J. Chem. Phys. Lett. 2000, 326, 454.
16. Gan, Z. J. Am. Chem. Soc. 2000, 122, 3242.
17. Brinkmann, D.; Staehli, J. L.; Ghose, S. J. Chem. Phys. 1969, 51, 5128.
18. Dollase, W. A. Am. Mineral. 1968, 53, 1882.
19. Ernst, H.; Freude, D.; Wolf, I. Chem. Phys. Lett. 1993, 212, 588.
20. Freude, D.; Ernst, H.; Wolf, I. Solid State Nucl. Magn. Reson. 1994, 3, 271.
21. Grey, C. P.; Vega, A. J. J. Am. Chem. Soc. 1995, 117, 8232.
22. Koller, H.; Meijer, E. L.; van Santen, R. A. Solid State Nucl. Magn. Reson. 1997, 9, 165.
23. Massiot, D.; Bessada, C.; Coutures, J. P.; Taulelle, F. J. Magn. Reson. 1990, 90, 231.
24. Chan, J. C. C. Conc. Magn. Reson. 1999, 11, 363.
25. Amoureux, J.-P.; Fernandez, C.; Frydman, L. Chem. Phys. Lett. 1996, 259, 347.
26. Amoureux, J.-P.; Fernandez, C. Solid State Nucl. Magn. Reson. 1998, 10, 211.
27. Samoson, A. Chem. Phys. Lett. 1985, 119, 29.
28. Samoson, A.; Lippmaa, E. Phys. Rev. B 1983, 28, 6567.
29. Massiot, D. J. Magn. Reson. A 1996, 122, 240.
30. Amoureux, J.-P.; Fernandez, C.; Steuernagel, S. J. Magn. Reson. A 1996, 123, 116.
31. Lee, S. K.; Stebbins, J. F. J. Phys. Chem. B 2000, 104, 4091.
32. Xu, Z.; Sherriff, B. L. Appl. Magn. Reson. 1993, 4, 203.