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note
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As indicated in Figure 1, the structure of the combination products III is not yet known completely. However, this does not invalidate any of our mechanistic conclusions that follow.
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35
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• is deprotonated under our experimental conditions.
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39
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In ref 5d
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Reference 15, p 67.
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2, 8.43 eV (Lias, S. G.; Bartmess, J. E.; Liebman, J. F.; Holmes, J. L.; Levin, R D.; Mallard, W. G. J. Phys. Chem. Ref. Data 1988, 17 (Suppl. 1)) and 8.63 eV (Aue, D. H.; Webb, H. M.; Bowers, M. I J. Am. Chem. Soc. 1976, 98, 311-317), respectively, indeed seem to indicate a preference of electron transfer from sulfur. However, the difference of these values is comparable to the precision of the measurements and the changes of the IPs with the substituents at S or N. Hence, we are reluctant to draw definitive conclusions from the IPs.
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2, 8.43 eV (Lias, S. G.; Bartmess, J. E.; Liebman, J. F.; Holmes, J. L.; Levin, R D.; Mallard, W. G. J. Phys. Chem. Ref. Data 1988, 17 (Suppl. 1)) and 8.63 eV (Aue, D. H.; Webb, H. M.; Bowers, M. I J. Am. Chem. Soc. 1976, 98, 311-317), respectively, indeed seem to indicate a preference of electron transfer from sulfur. However, the difference of these values is comparable to the precision of the measurements and the changes of the IPs with the substituents at S or N. Hence, we are reluctant to draw definitive conclusions from the IPs.
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56
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85033025165
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note
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•-.
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57
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85032998025
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note
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3d On the basis of our CIDNP data. we cannot distinguish between these alternatives. We are indebted to a referee for drawing our attention to this point.
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58
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0011688837
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