Synthesis, chemical characterization, X-ray crystal structure and magnetic properties of oxalato-bridged copper(II) binuclear complexes with 2,2′-bipyridine and diethylenetriamine as peripheral ligands

Polyhedron

Volumn 18, Issue 8-9, 1999, Pages 1235-1245

  Castillo, Oscar ^a   Muga, Iñaki ^a   Luque, Antonio ^a   Gutiérrez Zorrilla, Juan M ^a   Sertucha, Jon ^a   Vitoria, Pablo ^a   Román, Pascual ^a  

^a UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

Author keywords

Copper(II) complexes; Crystal structure; ESR; Magnetic properties; oxalato dimers

Indexed keywords

ATOMS; CHELATION; COPPER COMPOUNDS; CRYSTAL ATOMIC STRUCTURE; ELECTRON SPIN RESONANCE SPECTROSCOPY; LIGANDS; MAGNETIC MOMENTS; MAGNETIC SUSCEPTIBILITY; MOLECULES; NITRATES; OXYGEN; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); THERMOANALYSIS; X RAY DIFFRACTION;

BIPYRIDINES; CHEMICAL CHARACTERIZATION; COPPER ATOMS; COPPER(II) COMPLEX; CRYSTALS STRUCTURES; DIETHYLENETRIAMINE; ELECTRON-SPIN RESONANCE; OXALATO; OXYGEN ATOM; Μ-OXALATO DIMER;

DIMERS;

EID: 0000226037     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(98)00421-5     Document Type: Article

References (58)

1. R. Vicente, A. Escuer, J. Ferretjans, H. Stoeckli-Evans, X. Solans, M. Font-Bardía, J. Chem. Soc. Dalton Trans. (1997) 167.
2. S.G. Carling, C. Mathoniére, P. Day, K.M. Abdul-Malik, S.J. Coles, M.B. Hursthouse, J. Chem. Soc. Dalton Trans. (1996) 1839.
3. Decurtins S., Schmalle H.W., Pellaux R., Schneuwly P., Hauser A. Inorg. Chem. 35:1996;1451.
4. Sun X., Miao M., Cheng P., Liao D., Jiang Z., Wang G. Polyhedron. 15:1996;2927.
5. R. Vicente, A. Escuer, X. Solans, M. Font-Bardía, J. Chem. Soc. Dalton Trans. (1996) 1835.
6. J. Suárez-Varela, J.M. Dominguez-Vera, E. Colacio, J.C. Avila-Rosón, M.A. Hidalgo, D. Martín-Ramos, J. Chem. Soc. Dalton Trans. (1995) 2143.
7. De Munno G., Julve M., Nicolo F., Lloret F., Faus J., Ruiz R., Sinn E. Angew. Chem. Int. Ed. Engl. 32:1993;613.
8. Cleare M.J. Coord. Chem. Rev. 12:1974;349.
9. Sinha A., Shankar V. Ind. Eng. Chem. Res. 32:1993;1061.
10. Díaz-Guemes M.I., Bhatti A.S., Dollimore D. Thermochim. Acta. 110:1987;275.
11. Hauser A., Von Arx M.E., Pellaux R., Decurtins S. Mol. Cryst. Liq. Cryst. 286:1996;225.
12. Larionova J., Mombelli B., Sanchiz J., Khan O. Inorg. Chem. 37:1998;679.
13. Decurtins S., Schmalle H.W., Pellauz R., Huber R., Fischer P., Ouladdiaf B. Adv. Mater. 8:1996;647.
14. O. Kahn, Molecular magnetism. New York: VCH, 1993.
15. Kahn O. Angew. Chem. Int. Ed. Engl. 24:1985;834.
16. Román P., Guzmán-Miralles C., Luque A., Beitia J.I., Cano J., Lloret F., Julve M., Alvarez S. Inorg. Chem. 35:1996;3741.
17. Glerup J., Goodson P.A., Hodgson D.J., Michelsen K. Inorg. Chem. 34:1995;6255.
18. Oshio H., Nagashima U. Inorg. Chem. 31:1992;3295.
19. Girerd J.J., Khan O., Verdaguer M. Inorg. Chem. 19:1980;274.
20. Pellaux R., Schmalle H.W., Huber R., Fischer P., Hauss T., Ouladdiaf B., Decurtins S. Inorg. Chem. 36:1997;2301.
21. Coronado E., Galán-Mascarós J.R., Giménez-Saiz C., Gómez-García J., Ruiz-Pérez C., Triki S. Adv. Mater. 8:1996;737.
22. Pei Y., Journaux Y., Khan O. Inorg. Chem. 28:1989;100.
23. Alvarez S., Julve M., Verdaguer M. Inorg. Chem. 29:1990;4500.
24. Cano J., Alemany P., Alvarez S., Verdaguer M., Ruiz E. Chem. Eur. J. 4:1998;476.
25. Román P., Gutiérrez-Zorrilla J.M. J. Chem. Educ. 62:1985;167.
26. A. Earnshaw, Introduction to magnetochemistry. London: Academic Press, 1968.
27. F.S. Stephens, J. Chem. Soc. A (1969) 2493.
28. C. Guzmán-Miralles, PhD Thesis, Bilbao: Universidad del Pais Vasco, 1995.
29. K. Iron, W. Jeitschko, E. Parthe, LAZY PULVERIX. Laboratoire de Crystallographie aux rayons-X, Universtite of Geneve, 1977.
30. International tables for X-ray crystallography. Vol. IV. Birmingham: Kynoch Press, 1974.
31. P.T. Beurskens, G. Admiraal, G. Beurskens, W.P. Bosman, S. García-Granda, R.O. Gould, J.M.M. Smith, C. Smykalla, The DIRDIF program system. Technical report of the Crystallography Laboratory, University of Nijmegen, 1992.
32. Walker N., Stuart D. Acta Crystallogr. A39:1983;158.
33. J.M. Stewart, P.A. Machin, C.W. Dickinson, H.L. Ammon, H. Heck, H. Flack, The X-RAY76 system. Technical Report TR-446. Computer Science Center, University of Maryland, College Park, MD, 1976.
34. M. Martínez-Ripoll, F.H. Cano, Programa PESOS. Instituto Rocasolano, CSIC, Madrid, 1975.
35. Nardelli M. Comput. Chem. 7:1983;95.
36. Spek A.L. Acta Crystallogr. A46:1990;C34.
37. Li J.M., Sun J.Z., Chen P.C., Wu X.T. Cryst. Res. Tech. 30:1995;353.
38. Castro I., Faus J., Julve M., Muñoz M.C., Diaz W., Solans X. Inorg. Chim. Acta. 179:1991;59.
39. A. Gleizes, M. Julve, M. Verdaguer, J.A. Real, J. Faus, X. Solans, J. Chem. Soc. Dalton Trans. (1992) 3209.
40. L. Soto, J. García-Lozano, E. Escrivá, M. Beneto, F. Dahan, J.P. Tuchagues, J.P. Legros, J. Chem. Soc. Dalton Trans. (1991) 2619.
41. Soto L., García-Lozano J., Escrivá E., Legros J.P., Tuchagues J.P., Dahan F., Fuertes A. Inorg. Chem. 28:1987;3378.
42. B.J. Hathaway, in: G. Wilkinson (Ed.), Comprehensive coordination chemistry. Oxford: Pergamon, 1985, vol. V, p. 604 and references therein.
43. Hathaway B.J. Struct. Bonding (Berl.). 57:1984;55.
44. W. Fitzgerald, J. Foley, D. McSweeney, N. Ray, D. Sheahan, S. Tyagi, B.J. Hathaway, P. O'Brien, J. Chem. Soc. Dalton Trans. (1982) 1117.
45. Román P., Luque A., Guzmán-Miralles C., Beitia J.I. Polyhedron. 14:1995;2863.
46. J. Cano, G. de Munno, J. Sanz, R. Ruiz, F. Lloret, J. Faus, M. Julve, J. Chem. Soc. Dalton Trans. (1994) 3465.
47. A.W. Addison, T.N. Rao, J. Reedijk, J. Van Rijn, G.C. Verschoor, J. Chem. Soc. Dalton Trans. (1984) 1349.
48. Allmann A., Krestl M., Bolos C., Manoussakis G., Nikolov G.S. Inorg. Chim. Acta. 175:1990;255.
49. Britten J.F., Lock C.J.L. Acta Crystallogr. B36:1980;2958.
50. Julve M., Verdaguer M., Gleizes A., Philoche-Levisalles M., Kahn O. Inorg. Chem. 23:1984;3803.
51. Hall G.R., Duggan D.M., Hendrickson D.N. Inorg. Chem. 1975:1956;14.
52. Felthouse T.R., Laskowski E.J., Hendrickson D.N. Inorg. Chem. 16:1977;1077.
53. Bleaney B., Bowers K.D. Proc. R. Soc. London Ser. A. 214:1952;451.
54. Khan O., Briat B. J. Chem. Soc. Faraday Trans. 2:1976;268.
55. Girerd J.J., Charlot M.F., Khan O. Mol Phys. 34:1977;1063.
56. Bencini A., Fabretti A.C., Zanchini C., Zannini P. Inorg. Chem. 26:1987;1445.
57. Sletten J. Acta Chem. Scand. A37:1983;569.
58. Henke W., Kremer S., Reinen D. Inorg. Chem. 22:1983;2858.