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Volumn 28, Issue 10, 1987, Pages 1031-1034

Asymmetric aza-Claisen rearrangement: Synthesis of (+)-dihydropallescensin-2 [(+)-penlanpallescensin].

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Indexed keywords


EID: 0000161770     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)95903-3     Document Type: Article
Times cited : (39)

References (22)
  • 7
    • 84919090008 scopus 로고    scopus 로고
    • (S)-(-)-4,5-Dihydro-2-methyl-4-(1-methylethyl)oxazole (5) was prepared in enantiomerically pure from commercially available L-2-amino-3-methyl-1-butanol as described in ref. 2.
  • 9
    • 84919090007 scopus 로고    scopus 로고
    • This diastereomer ratio was determined with a 5890A Hewlett·Packard GC using a 15 m x 0.33 mm i.d. DB-1701 fused silica capillary column with a flame ionization detector, helium carrier gas (50 cm/sec), 200°C injector temperature, column oven temperature programmed at 105°C isotherm, and 3390A Hewlett·Packard integrator: 10s at 27.82 min and 10r at 28.58 min.
  • 11
    • 84919090006 scopus 로고    scopus 로고
    • 3); mass [[Truncated]]
  • 14


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.