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Journal of Organic Chemistry

Volumn 61, Issue 19, 1996, Pages 6735-6738

Bis-allylic templates for Pd(0)-catalyzed solid phase synthesis of tertiary amines

(2) Flegelová, Zuzana a Pátek, Marcel a

a Selectide Corporation (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000141965 PISSN: 00223263 EISSN: None Source Type: Journal
DOI: 10.1021/jo960756+ Document Type: Article

Times cited : (27)

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- 85033867596
- note
- 19F NMR spectra of N-(4-fluorobenzyl)-N-(3-(tetrahydroisoquinolino)-2-methylenepropyl)glycine and N-(4-fluorobenzyl)-N-(benzylamino)-2-methylenepropyl)glycine revealed the stoichiometry corresponding to bis-trifluoroacetates after the preparative HPLC. Isolated yields are therefore based on stoichiometric amounts of trifluoroacetic acid per amine functionality.

53
- 85033870462
- note
- The purities of compounds 6, 7a-1 were calculated from integrated peak areas recorded by the HPLC analysis (215 nm) of the crude product which was cleaved from the solid support after complete conversion of the starting material.

54
- 0028921695
- (a) Doi, T.; Yanagisawa, A.; Miyazawa, M.; Yamamoto, K. Tetrahedron: Asymmetry 1995, 6, 389-392.
- (1995) Tetrahedron: Asymmetry , vol.6 , pp. 389-392
- Doi, T.¹ Yanagisawa, A.² Miyazawa, M.³ Yamamoto, K.⁴

55
- 0028835937
- (b) Lemaire-Audoire, S.; Savignac, M.; Genet, J. P.; Bernard, J. M. Tetrahedron Lett. 1995, 36, 1267-1270.
- (1995) Tetrahedron Lett. , vol.36 , pp. 1267-1270
- Lemaire-Audoire, S.¹ Savignac, M.² Genet, J.P.³ Bernard, J.M.⁴

56
- 85033836461
- note
- 2-allylic protons.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.