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Volumn 17, Issue 22, 1976, Pages 1849-1852

Organolithium reagents from alkyl halides and lithium DI-tert-butylbiphenyl

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000137721 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)92942-3 Document Type: Article

Times cited : (70)

References (19)

2
- 8644288985
- (1966) J. Amer. Chem. Soc. , vol.88 , pp. 4260
- Garst¹ Ayers² Lamb³

3
- 0006598563
- Radical Intermediates in the Oxygenation of a Grignard Reagent
- (1966) Journal of the American Chemical Society , vol.88 , pp. 4261
- Cristol¹ Barbour²

11
- 37049130364
- Stoicheiometry and synthetic utility of the reaction of alkyl halides with lithium dihydronaphthylide
- Only two reports of the use of LiN to form simple alkyllithium reagents have appeared in the literature
- (1972) Journal of the Chemical Society, Chemical Communications , pp. 752
- Scettas¹

12
- 0006541826
- (1973) J. Amer. Chem. Soc. , vol.95 , pp. 8201
- Zieger¹ Anges² Maresca³

13
- 0344695838
- (1975) J. Amer. Chem. Soc. , vol.97 , pp. 3313
- Shimada¹ Szwarc²

14
- 84918021443
- The EST spectra of potassium di-t-butylbiphenyl has been measured by M.D. Curtis and A.L. Allred, J. Amer. Chem. Soc., 87, 2554 (1965)

15
- 84918021442
- The lithium di-tert-butylbiphenyl solution is formed by adding slivers of lithium directly to a solution of slightly greater than on equivalent of DBB in THF under a flow of argon. The deep blue color of the radical anion forms immediately, if water, oxygen and carbon dioxide have been excluded. The solution is cooled to 0° and stirred until the reaction is complete. The resulting solution of LiDBB will decompose slowly at room temperature.

16
- 0003909903
- Pergamon Press, Elmsford, N.Y
- (1974) The Chemistry of Organolithium Compounds , pp. 21
- Wakefield¹

18
- 84918021441
- The mixture of syn and anti-7-chloronorcaranes reacs a little more slowly, requiring about 30 sec for complete reaction.

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