Heteroleptic polypyrazolylborate complexes of the lanthanides: Syntheses and molecular structures of [Nd{HB(pz)3}2Cl(H2O)] (HB(pz)3=hydrotris(pyrazol-1-yl)borate) and [Nd{HB(pz*)3}LCl2] (HB(pz*)3=hydrotris(3,5-dimethylpyrazol-1-yl)borate; L=4,4′-di-tert-butyl-2,2′-bipyridine)

Inorganica Chimica Acta

Volumn 255, Issue 2, 1997, Pages 355-360

  Sun, Chao De ^a   Wong, Wing Tak ^a  

^a UNIVERSITY OF HONG KONG   (Hong Kong)

Author keywords

Crystal structures; Heteroleptic polypyrazolylborate complexes; Lanthanide complexes

Indexed keywords

CHLORINE COMPOUNDS; CRYSTAL STRUCTURE; MOLECULAR STRUCTURE; RARE EARTH ELEMENTS; SPECTROSCOPIC ANALYSIS; SYNTHESIS (CHEMICAL); X RAY CRYSTALLOGRAPHY;

BIPYRIDINES; CONVENTIONAL SPECTROSCOPIC METHODS; HETEROLEPTIC; LANTHANIDE COMPLEX; POLYPYRAZOLYLBORATES;

NEODYMIUM COMPOUNDS;

EID: 0000082619     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/s0020-1693(96)05392-3     Document Type: Article

References (29)

1. C. Schaverien, Adv. Organomet. Chem., 36 (1994) 283.
2. S. Trofimenko, Chem. Rev., 93 (1993) 943.
3. S. Trofimenko, Prog. Inorg. Chem., 34 (1986) 115.
4. K.W. Bagnall, A.C. Tempest, J. Takats and A.P. Masino, Inorg. Nucl. Chem. Lett., 12 (1976) 555.
5. M.V.R. Stainer and J. Takats, Inorg. Chem., 21 (1982) 4050.
6. D.L. Reger, J.A. Lindeman and L. Lebioda, Inorg. Chim. Acta, 139 (1987) 71.
7. (a) M.A.J. Moss, C.J. Jones and A.J. Edwards, Polyhedron, 7 (1988) 79;
8. (b) M.A.J. Moss and C.J. Jones, J. Chem. Soc., Dalton Trans., (1989) 1393.
9. D.L. Reger, J.A. Lindeman and L. Lebioda, Inorg. Chem., 27 (1988) 3923.
10. M.A.J. Moss and C.J. Jones, Polyhedron, 8 (1989) 117.
11. (a) M.A.J. Moss and C.J. Jones, Polyhedron, 8 (1989) 555;
12. (b) J. Chem. Soc., Dalton Trans., (1990) 581.
13. D.L. Reger, S.J. Knox, J.A. Lindeman and L. Lebioda, Inorg. Chem., 29 (1990) 416.
14. M.A.J. Moss and C.J. Jones, Polyhedron, 8 (1989) 2367.
15. M.A.J. Moss and C.J. Jones, Polyhedron, 9 (1990) 697.
16. M.A.J. Moss and C.J. Jones, Polyhedron, 8 (1989) 117.
17. J. Takats, X.W. Zhang, V.W. Day and T.A. Eberspacher, Organometallics, 12 (1993) 4286.
18. S.Y. Liu, G.H. Maunder, A. Sella, M. Stevenson and D.A. Tocher, Inorg. Chem., 35 (1996) 76.
19. D.L. Reger, M.E. Tarquini and L. Lebioda, Organometallics, 2 (1983) 1763.
20. D.L. Reger, R. Mahtab, J.C. Baxter and L. Lebioda, Inorg. Chem., 25 (1986) 2046.
21. Y.K. Gun'ko, P.B. Hitchcock and M.F. Lappert, J. Organomet. Chem., 499 (1995) 213.
22. W. Chen, Z. Jin, Y. Xing, Y. Fan and G. Yang, Inorg. Chim. Acta, 130 (1987) 125.
23. D.D. Perrin, W.L.F. Armarego and D.R. Perrin, Purification of Laboratory Chemicals, Pergamon, Oxford, 1980.
24. S. Trofimenko, J. Am. Chem. Soc., 89 (1967) 6288.
25. S. Trofimenko, J. Am. Chem. Soc., 89 (1967) 3170.
26. F.A. Hart and J.E. Newbery, J. Inorg. Nucl. Chem., 31 (1969) 1725.
27. A.C.T. North, D.C. Phillips and F.S. Mathews, Acta Crystallogr., Sect. A, 24 (1968) 351.
28. M.C. Burla, M. Camalli, G. Cascarano, C. Giacovazzo, G. Polidori, R. Spagna and D. Viterbo, J. Appl. Crystallogr., 22 (1989) 389.
29. TeXsan: Crystal Structure Analysis Package, Molecular Structure Corporation, The Woodlands, TX, 1985 and 1992.