29Si and 13C NMR Investigation of the Polysilane-to-Poly(carbosilane) Conversion of Poly(methylchlorosilanes) Using Cross-Polarization and Inversion Recovery Cross-Polarization Techniques

Chemistry of Materials

Volumn 8, Issue 7, 1996, Pages 1415-1428

  Babonneau, Florence ^a   Maquet, Jocelyne ^a   Bonhomme, Christian ^a   Richter, Robin ^b   Roewer, Gerhard ^b   Bahloul, Djamila ^c  

^a SORBONNE UNIVERSITÉ   (France)

^b TU BERGAKADEMIE FREIBERG   (Germany)

^c UNIVERSITY OF LIMOGES   (France)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000060152     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm960002b     Document Type: Article

References (41)

1. Brinker C. J.; Scherrer, G. W. Sol-Gel Science; Academic Press: New York, 1990.
2. Wynne, K. J.; Rice, R. W. Annu. Rev. Mater. Sci. 1984, 14, 297.
3. Pouskouleli, G. Ceram. Int. 1989, 15, 213.
4. Peuckert, M.; Vaahs, T.; Brück, M. 1990, 2, 398.
5. Laine, R. M.; Babonneau, F. Chem. Mater. 1993, 5, 260.
6. Yajima, S.; Hayashi, J.; Omori, M. Chem. Lett. 1975, 931.
7. Yajima, S. In Handbook of Composites; Watt, W., Perov, B. V., Eds.; Elsevier Science Publishers: Dordrecht, 1985; Vol. 1, p 201.
8. Gérardin, C.; Henry, M.; Taulelle, F. In Better Ceramics through Chemistry V; Hampden-Smith, M. J., Klemperer, W. G., Brinker, C. J., Eds.; Mat. Res. Soc. Symp. Proc. Vol. 271, 1992; p 777.
9. Sorarù, G. D.; Babonneau, F.; Mackenzie, J. D. J. Mater. Sci. 1990, 25, 3886.
10. Schmidt, W. R.; Interrante, L. V.; Doremus, R. H.; Trout, T. K.; Marchetti, P. S.; Maciel, G. E. Chem. Mater. 1991, 3, 257.
11. Derome, A. E. Modern NMR Techniques for Chemistry Research; Pergamon Press: New York, 1987.
12. Alia, M.; Lippmaa, E. Chem. Phys. Lett. 1976, 37, 260.
13. Opella, S. J.; Frey, M. H. J. Am. Chem. Soc. 1979, 101, 5854.
14. Cory, D. G.; Ritchey, W. M. Macromolecules 1989, 22, 1611.
15. Tekely, P.; Montigny, F.; Canet, D.; Delpuech, J. J. Chem. Phys. Lett. 1990, 175, 401.
16. Wu, X.; Zilm, K. W. J. Magn. Reson. 1993, A102, 205.
17. Palmas, P.; Tekely, P.; Canet, D. J. Magn. Reson. 1993, A104, 26.
18. Sangill, R.; Rastrup-Andersen, N.; Bildsoe, H.; Jakobsen, H. J.; Nielsen, N. C. J. Magn. Reson. 1994, A107, 67.
19. Wu, X.; Zhang, S. Chem. Phys. Lett. 1989, 156, 79.
20. Alemany, L. B.; Grant, D. M.; Pugmire, R. J.; Alger, T. D.; Zilm, K. W. J. Am. Chem. Soc. 1983, 105, 2142.
21. Hirschinger, J.; Hervé, M. Solid State Magn. Reson. 1994, 3, 121.
22. Wu, X.; Burns, S. T.; Zilm, K. W. J. Magn. Reson. 1994, A111, 29.
23. Bonhomme, C.; Maquet, J.; Livage, J.; Mariotto, G. Inorg. Chim. Acta 1995, 230, 85.
24. Zumbulyadis, N. J. Chem. Phys. 1987, 86, 1162.
25. Bonhomme, C.; Babonneau, F.;Maquet, J.; Livage, J.; Vaultier, M.; Framery, E. J. Chim. Phys. 1995, 92, 1881.
26. Herzog, U.; Richter, R.; Brendler, E.; Roewer, G. J. Organomet. Chem. 1996, 507, 221.
27. Brendler, E.; Leo, K.; Thomas, B.; Richter, R.; Roewer, G.; Krämer, H. In Organosilicon Chemistry II; Auner, N., Weis, J., Eds.; VCH: Weinheim, 1996; p 69.
28. Watanabe, H.; Kobayashi, M.; Koike, Y.; Nagashima, S.; Nagai, Y. J. Organomet. Chem. 1977, 128, 173.
29. Albrecht, J.; Richter, R.; Roewer, G. Patent DE 42 07 299 A1, 1993.
30. Richter, R. Dissertation, Technischen Universität Bergakademie Freiberg, Germany, 1995.
31. Richter, R.; Roewer, G.; Böhme, U.; Busch, K.; Babonneau, F.; Martin, H. P.; Müller, E. Appl. Organomet. Chem., submitted.
32. Massiot, D.; Thiele, H.; Germanus, A. Bruker Rep. 1994, 140, 43.
33. Pines, A.; Gibby, M. G.; Waugh, J. S. J. Chem. Phys. 1973, 59, 569.
34. Müller, L.; Kumar, A.; Baumann, T.; Ernst, R. R. Phys. Rev. Lett. 1974, 32, 1402.
35. Alemany, L. B.; Grant, D. M.; Alger, T. D.; Zilm, K. W. J. Am. Chem. Soc. 1983, 105, 6697.
36. Alemany, L. B.; Grant, D. M.; Pugmire, R. J.; Alger, T. D.; Zilm, K. W. J. Am. Chem. Soc. 1983, 105, 2133.
37. Tekely, P.; Gérardy, V.; Palmas, P.; Canet, D.; Retournard, A. Solid State Nucl. Magn. Reson. 1995, 4, 361-367.
38. Wu, H.-J.; Interrante, L. V. Chem. Mater. 1989, 1, 564.
39. Yajima, S.; Hasegawa, Y.; Hayashi, J.; limura, M. J. Mater. Sci. 1978, 13, 2569.
40. Marsmann, H. In NMR Basic principles and Progress; Dielh, P., Fluck, E., Kosfeld, R., Eds.; Springer Verlag: Heidelberg, 1981; Vol. 17.
41. Sakurai, H.; Koh, R.; Hosomi, A.; Kumada, M. Bull. Chem. Soc. Jpn. 1966, 39, 2050.